Scott's advice is good. I'd also follow up by suggesting that if you have any questions about compliance at your station that you participate in the Alternative Broadcast Inspection Program. I'm assuming you are in New Jersey - the New Jersey Broadcaster's Association administers the program in the state. You pay a fee, a consulting engineer comes in and inspects your operation. If there are compliance issues, you are advised as to how to address them. If found to be in compliance, you get a certificate. Hang it in your lobby and the FCC will not inspect your station on a "random" basis for the validity period of the certificate. They may still inspect as part of a targeted compliance issue or complaint, but the ABIP certificate provides good peace of mind that you're in substantial compliance.
I also recommend reading the rules themselves. 47 CFR 73.1870 specifies the rules regarding Chief Operators and 73.1800 and 73.1820 specify rules regarding the Station Log. You can also follow the FCC Self-Inspection Checklist.
The big compliance issues are the following:
EAS: Are you monitoring the correct stations as listed in the State Plan? Have you been receiving tests or activity from required monitor sources weekly? If not, you need to research the cause of any missed tests and log the cause. Are you relaying required-relay items? Are you issuing Required Weekly Tests? Any missing activity - either receiving or transmitting - without explanation is cause for a violation. You must have a copy of the current FCC EAS Handbook available at the Primary Control Point.
Public File: This is a whole section on its own. For a non-comm, go through the list in 73.3527 (e). Any missing documents are a violation.
Chief Operator: You must have a written designation of Chief Operator. This goes at the posting point with your station licenses. The Chief Operator is required to review the Station Log weekly and sign and date it. The Station Log does not necessarily have to contain "meter readings" as it used to - though such readings are a part of the Station Log when taken - but you have to review and sign something weekly. Nowadays this is mostly EAS and tower light monitoring.
Antenna Structure Registration: If you own the tower and it's required to be registered, the registration must be correct and the ASRN must be posted as required. Note that the FCC is writing up stations for administrative violations related to ASRNs such as towers showing as "under construction" or an outdated registrant address or phone number.
Tower marking: Your tower lights must be working and paint must be in good condition if required. If you are the tower owner, it is your responsibility. If you are a licensee on the tower, you may be held responsible if the owner doesn't do it. Tower lights must be monitored. Quarterly tower lighting inspections are required.
AM station tower fencing: Effective locked fences are required at any AM tower with potential at the tower base. You must have a key to the fence. Fencing in poor condition, easily bypassed, or too small to prevent access to the tower is a violation.
Main studio rules: Your station must have a main studio located within your community of license, within the primary service contour of any other AM, FM, or TV station with the same community of license, within 25 miles of the reference coordinates of the community of license, or you must have a waiver. The main studio must be staffed by one full-time management-level employee and one part-time employee or more during business hours. You must have a telephone number that is toll-free to the community of license.
Equipment performance measurements: For an FM you must retain your most recent Equipment Performance Measurement for inspection. For an AM you must complete annual NRSC measurements.
RFR: You must comply with standards protecting the general public and workers from excessive Radio Frequency Radiation conditions.
Auxiliary Service licensing: If you are operating any stations in the Broadcast Auxiliary Service (microwave STLs, RPUs, etc.) you must operate those stations in accordance with their authorizations and maintain copies of those authorizations.
FCC rules may be read here:
http://www.hallikainen.com/FccRules/2010/73/
If you need assistance with compliance or other technical matters, I am available for such services in New York or New Jersey.